Bu oar's
WebThe use of a tailored complex 3 where one of the aryloxides is replaced with a more reactive pyrrolyl ligand significantly increases the selectivity of grafting leading to the formation of the Ti... WebDownload scientific diagram Synthesis of [OC t Bu 3 ] and [OC t Bu 2 Ph] ligand precursors. from publication: Discrete Complexes of 3d Metals with Monodentate Bulky Alkoxide Ligands and Their ...
Bu oar's
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WebApr 1, 2024 · For [Ln(OAr) 3] (Ar = 2,6-t Bu 2-4-RC 6 H 2), the preference to be pyramidal is stronger than for Y. As the Ln–O bond length shortens, the increase in energy induced by the trend towards planarity (owing to the steric repulsion between bulky ligands) is balanced by an additional C–H⋯Ln interaction. Webalkoxy-NHC metallated product is indeed obtained with Al(iBu) 3. In contrast, the sterically hindered [Al(iBu)(OAr) 2] (OAr = 2,6-di-tertbutyl-4-methylphenoxy) displays reactivity at the carbene and affords an imidazolium-aluminate zwitterion. The non-innocence of the Al-NHC motif is further highlighted by the heterolytic cleavage
WebReaction of the nitride with trimethylsilyl trifluoromethanesulfonate afforded the monomeric trimethylsilyl imido species, W(NSiMe3)(CH2-t-Bu)(OAr)2(OSO2CF3), which was also characterized ...
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